Xylem TitroLine 7000 Manual De Instrucciones página 125

TABLE OF CONTENT
1 Technical Specifications of the Titrator TitroLine
1.1 Notes to the operating manual .............................................................................................. 127
1.2 Intended Use ......................................................................................................................... 127
1.3 Technical Specifications ........................................................................................................ 128
1.3.1 Titrator TitroLine
1.4 Warning and safety information ............................................................................................ 131
2 Installation and Commissioning......................................................................... 132
2.1 Unpacking and setting up ...................................................................................................... 132
2.2 Back panel of the titrator TitroLine
2.3 Connection and installation of the titrator and the magnetic stirrer TM235/TM235 KF ........ 134
2.4 Installation of the Z 300 Rod Foot Plate (Optional) ............................................................... 134
2.5 Setting the language ............................................................................................................. 135
2.7 Exchangeable head (WA) ..................................................................................................... 136
2.7.1 Installation of the Interchangeable Unit ................................................................................. 136
2.7.2 Placing and Replacing of the Interchangeable Unit .............................................................. 137
2.7.3 Programming of the titration unit ........................................................................................... 138
2.7.4 Initial Filling or Rinsing of the Entire Interchangeable Unit ................................................... 140
2.8 Installing the burette tip ......................................................................................................... 142
2.9 Replacing the Glass Cylinder and the PTFE Piston ............................................................. 143
2.10 Combination with Accessories and Additional Devices ........................................................ 144
2.10.1 Connecting a printer .............................................................................................................. 144
2.10.2 Connecting a USB device ..................................................................................................... 144
2.10.3 Connection of analytical balances ......................................................................................... 144
2.10.4 Connection of SI Analytics
3 Working with the Titrator TitroLine
3.1 Front Keyboard ...................................................................................................................... 145
3.2 Display ................................................................................................................................... 145
3.3 Manual controller ................................................................................................................... 146
3.4 External PC Keyboard ........................................................................................................... 146
3.5 Menu Structure ...................................................................................................................... 147
3.6 Main Menu ............................................................................................................................. 149
3.6.1 Automatic Titration ................................................................................................................ 149
3.6.2 Calibration (CAL-Menü)......................................................................................................... 151
3.6.3 Manual Titration ..................................................................................................................... 154
3.6.4 Dosage .................................................................................................................................. 156
3.6.5 Preparing Solutions ............................................................................................................... 158
4 Method parameters.............................................................................................. 159
4.1 Method editing and new method ........................................................................................... 159
4.2 Default method ...................................................................................................................... 160
4.3 Copy Method ......................................................................................................................... 160
4.4 Delete Method ....................................................................................................................... 161
4.5 Print method .......................................................................................................................... 161
4.6 Change Method Parameters ................................................................................................. 162
4.6.1 Method type ........................................................................................................................... 162
4.6.2 Titration mode ....................................................................................................................... 162
4.6.3 Result .................................................................................................................................... 165
4.6.4 Formula Editor ....................................................................................................................... 176
4.6.5 Titration parameters .............................................................................................................. 182
"End-Point titration" and "Dead-Stop titration" titration parameters ...................................... 190
4.6.6
4.6.7 Titration parameter pH-Stat Titration ..................................................................................... 191
4.6.8 Dosing parameter .................................................................................................................. 195
4.6.9 Sample identification ............................................................................................................. 196
4.6.10 Documentation ...................................................................................................................... 197
4.7 Measuring method ................................................................................................................. 198
5 Dosing and titration with externally connected piston burettes and titrators 200
5.1 Requirements ........................................................................................................................ 200
5.2 Dose with external piston burettes/titrators ........................................................................... 200
5.2.1 Titration with external piston burettes/titrators ...................................................................... 206
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7000 ......................................................................................................... 128
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7000 ............................................................................. 133
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ID electrodes............................................................................. 144
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7000 .................................. 127
7000 ......................................................... 145